Ensolisation-silylation reaction study of selected steroids.
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Date
Authors
Hehenberger, Anna
null, null
Kotas, Petr
Tříska, Jan
Journal Title
Journal ISSN
Volume Title
Publisher
Institute of Analytical Chemistry AS CR, v.v.i.
Abstract
For the purposes of trace analysis of 1,4-androstadiene-3,17-dione (ADD), 1,4-androstadiene-3-one-17β-ol (Boldenone) and 17-β-estradiol in water, waste water, soil and for the further phytosterols transformation studies the enolisation-silylation reaction was studied using MSTFA and BSTFA with different catalysts as derivatization reagents. The different reaction conditions and stability of the products was also studied using GC-MS technique.